U.S. flag

An official website of the United States government, Department of Justice.

Linking Ammonium Nitrate – Aluminum (AN-AL) Post-Blast Residues to PreBlast Explosive Materials Using Isotope Ratio and Trace Elemental Analysis for Source Attribution

NCJ Number
309919
Date Published
2024
Length
20 pages
Annotation

This publication reports the preliminary findings from a field study to recover samples of post-blast explosives from controlled detonations for the development of forensic examinations that can attribute signatures from post-blast debris to the signatures of pre-blast explosive materials for use in future investigations.

Abstract

The field study reported in this paper was conducted in order to provide proof-of-concept for the development of forensic examination methodologies that can attribute signatures from post-blast debris to signatures in pre-blast explosive materials. The project aimed to recover samples of post-blast explosives from controlled detonations of ammonium nitrate-aluminum (AN-AI) which were analyzed via isotope mass spectrometry (IRMS) and inductively-coupled plasma mass spectrometry (ICP-MS) for quantification and profiling of isotopes ratio and trace element signatures. Trace element results from AN-AI support the findings of the isotope ratio data, with 26 elements detected in both pre- and post-blast samples, and several elements, including B, Cd, Cr, Ni, Sn, V, and Zn showing considerable overlap.

Date Published: January 1, 2024